Synthesis and structural and morphological characterization of ZnO2 nanoparticles assisted with UV for bactericidal applications

Authors

  • Roberto Colonia Science Faculty, National Engineering University. Lima, Peru
  • Vanessa C. Martinez Science Faculty, National Engineering University. Lima, Peru.
  • José L. Solís Science Faculty, National Engineering University. Lima, Peru.
  • Mónica Gómez León Science Faculty, National Engineering University. Lima, Peru. https://orcid.org/0000-0003-0990-0593

DOI:

https://doi.org/10.21754/tecnia.v23i1.63

Keywords:

Zinc peroxide, Nanoparticles, Bactericidal

Abstract

 

Zinc peroxide (ZnO2) nanoparticles were synthesized by sol-gel technique. The chemicals used for the synthesis were zinc acetate di-hydrate (Zn(CH3COO)2.2H2O) and hydrogen peroxide (H2O2) at 30% under UV radiation. The structure of the ZnO2 nanoparticles was characterized by X-ray diffraction. While the morphology and the cluster size, were determined using scanning electron microscopy. For a preliminary evaluation of the bactericidal properties of the ZnO2, the material was exposed to Bacillus subtilis (ATCC 6051), Escherichia coli (ATCC 25922) y Staphylococcus aureus (ATCC 25923) and it was found that the material has notorious antibacterial activity. 

Downloads

Download data is not yet available.

References

[1] Chen, W., et al., "Synthesis, Thermal Stability and Properties of ZnO2 Nanoparticles". J. Phys. Chem. C., 2009. 113: p. 1320-1324.

[2] Ibarra, L., Alzorriz, M., "Effect of Temperature on the Crosslink Densities of Nitrile Rubber and Carboxylated Nitrile Rubber with Zinc Peroxide". Journal of Applied Polymer Science, 2002. 86: p. 335–340.

[3] Ibarra, L., Marcos-Fernández, A., Alzorriz, M., "Mechanistic approach to the curing of carboxylated nitrile rubber (XNBR) by zinc peroxide/zinc oxide". Polymer, 2002. 43: p. 1649-1655.

[4] Ibarra, L., Alzorriz, M., "Ionic Elastomers Based on Carboxylated Nitrile Rubber (XNBR) and Zinc Peroxide: Influence of Carboxylic Group Content on Properties". J. of Appl. Polymer Science, 2002. 84: p. 605- 615.

[5] Ohno, S., Aburatani, N., Ueda, N., "Blowing Composition". 1981: U.S.

[6] Hagel, R., "Verwendung von Zinkperoxid als Oxidationsmittel für Sprengstoffe und Pyrotechnische Gemische E". Patentschrift, Editor. 1984.

[7] Meleney, F. L., Harvey, H. D., "The Combined use of zinc peroxide and sulfanilamide in the treatmnet of chronic, undermining, burrowing ulcers due to the micro-Aerophilic Hemolytic Streptococcus". Annals of Surgery 1939: p. 1067-1094.

[8] Meleney, F. L., "Zinc Peroxide in Surgical Infections". The American Journal of Nursing, 1941. 41(6): p. 645-649.

[9] Johnson, B. A., Meleney, F. L., "The antiseptic and detoxifying action of zinc peroxide on certain surgical aerobic, anaerobic and micro-Aerophilic Bacteria". Annals of Surgery, 1939. 109(6).

[10] Hsu, C.-C., Wu, N. L., "Synthesis and photocatalytic activity of ZnO/ZnO2 composite". Journal of Photochemistry and Photobiology A: Chemistry, 2005. 172: p. 269–274.

[11] Sun, M., et al., "A simple and green approach for preparation of ZnO2 and ZnO under sunlight irradiation". Chemical Physics Letters, 2007. 443: pp. 342–346.

[12] Uekawa, N., et al., "Synthesis of ZnO Nanoparticles by Decomposition of Zinc Peroxide". Chemistry Letters, 2001: pp. 606- 607.

[13] Uekawa, N., et al., "Nonstoichiometric properties of zinc oxide nanoparticles prepared by decomposition of zinc peroxide". Phys. Chem. Chem. Phys., 2003. 5: pp. 929–934.

[14] Cheary, R. W., Coelho, A., "A Fundamental Parameters Approach to X-ray Line-Profile Fitting". J. Appl. Cryst, 1992. 25: p. 109-121.

[15] Young, R. A., "The Rietveld Method". 2002, United States: Oxford University Press.

[16] Chapman, J., Sullivan, T., Regan, F., "Nanoparticles in Anti-Microbial Materials

Published

2013-06-01

How to Cite

[1]
R. Colonia, V. C. Martinez, J. L. Solís, and M. Gómez León, “Synthesis and structural and morphological characterization of ZnO2 nanoparticles assisted with UV for bactericidal applications”, TECNIA, vol. 23, no. 1, pp. 17–23, Jun. 2013.

Issue

Section

Articles