Estimation of the uncertainty in the barium analytical technique in wastewater by atomic absorption spectrometry
DOI:
https://doi.org/10.21754/tecnia.v23i1.65Keywords:
Atomic absorption spectrometer, Barium, Uncertainty, Waste water, ISO/IEC 17025:2005Abstract
This paper aims to estimate the measurement uncertainty of the method Standard Methods 3111 D - Direct Nitrous Oxide - Acetylene Flame Method for the determination of barium in the wastewater matrix by atomic absorption spectrometry, using a model estimation uncertainty factors as requested by the guideline INDECOPI-acr-09 CRT-D, low approach quality management system of testing laboratories ISO / IEC 17025:2005.
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[1] BIPM/IEC/IFCC/ISO/IUPAC/IUPAP/OIML, “Guide to the expression of uncertainty in measurement “, GUM (1993).
[2] ISO-TS 21748:2004, IDT, “Guidance for the use of repeatability, reproducibility and trueness estimates in measurement uncertainty estimation”.
[3] DIRECTRIZ CRT-acr-09-D, “Directriz para la estimación y expresiónde la incertidumbre de la medición”, Versión 00, 2008.
[4] EURACHEM/CITAC Guide –“Quantifying Uncertainty in Analytical Measurement”– Third Edition 2012.
[5] Adams, T. M., “Guide for estimation of measurement uncertainty in testing”, A2LA, 2002.
[6] Puglisi, C., Kornblit, F., “Incertidumbre de medición en química analítica. Recta de calibración”. Buenos aires, Argentina.
[7] Perruchet, C., Priel, M., “Estimacion de la incertidumbre, medidas y ensayos”. AENOR, España 2000.
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